Synthesis of 4-(tert-Butyldimethylsilyl)-4,5,6,7-tetrahydro-[1,2,3]triazolo[1,5-a]pyridine by Rasma Kroņkalne Rūdolfs Beļaunieks & Māris Turks
![Synthesis of 4-(tert-Butyldimethylsilyl)-4,5,6,7-tetrahydro-[1,2,3]triazolo[1,5-a]pyridine by Rasma Kroņkalne Rūdolfs Beļaunieks & Māris Turks](https://img.ebook-hunter.org/img/Synthesis%20of%204-%28tert-Butyldimethylsilyl%29-4%2C5%2C6%2C7-tetrahydro-%5B1%2C2%2C3%5Dtriazolo%5B1%2C5-a%5Dpyridine%20by%20Rasma%20Kro%C5%86kalne%20R%C5%ABdolfs%20Be%C4%BCaunieks%20%26%20M%C4%81ris%20Turks.jpg)
Author:Rasma Kroņkalne, Rūdolfs Beļaunieks & Māris Turks
Format: pdf
Tags: SN2 rection between 4-(tert-butyldimethylsilyl)hex-5-yn-1-yl 4-methylbenzenesulfonate and NaN3 in DMF at 80 C provided (6-azidohex-1-yn-3-yl)(tert-butyl)dimethylsilane intermediate, which underwent in situ intramolecular thermal Huisgen azide–alkyne cycloaddition reaction. This one-pot process gave 4-(tert-butyldimethylsilyl)-4,5,6,7-tetrahydro-[1,2,3]triazolo[1,5-a]pyridine in 78% yield., triazole; triazolopyridine; Huisgen thermal cycloaddition; azide; intramolecular cyclization
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