Clinical Applications of Mass Spectrometry in Biomolecular Analysis by Uttam Garg

Author:Uttam Garg
Language: eng
Format: epub
Publisher: Springer New York, New York, NY

We describe here a rapid method for the selective analysis of MMA in serum, plasma , and urine that is based on unique fragmentation of di-butyl MMA combined with a mathematical deconvolution approach, which allows quantitation of MMA in the presence of SA without chromatographic separation. The instrumental analysis time of this method is 1 min per sample.

2 Materials

2.1 Samples

1.Serum (serum or serum separator tube) and plasma (sodium heparin or EDTA). Samples are stable for 4 days if refrigerated or 6 months frozen at or below −20 °C.

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