Nanoscience and Nanotechnology in Security and Protection against CBRN Threats by Unknown

Author:Unknown
Language: eng
Format: epub
ISBN: 9789402420180
Publisher: Springer Netherlands

19.2.2 DSC Measurements

Differential scanning calorimetry (DSC) analyses were carried out on a Q200 TA Instruments calibrated with indium, with 10 K/min under inert atmosphere: First, we made a heating scan from 303 to 503 K to investigate thermal transition to the drop-casted material and, in order to erase the thermal history of the samples, we stabilized the temperature at 503 K for 5 minutes. Then we started the measurements of cooling scan till 303 K to identify the thermal transition of relaxed nanocomposites material at the different C-Dots loading. A reheating scan from 303 to 503 K allowed recognizing the thermal transitions with the same thermal history [21]. Glass transitions are evident in the cooling and in the second heating scan.

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