Clinical Applications of Mass Spectrometry in Drug Analysis by Uttam Garg
Author:Uttam Garg
Language: eng
Format: epub
Publisher: Springer New York, New York, NY
(b)Evaporate to dryness for 20 min at 37 °C on the Turbovap.
(c)Reconstitute with 0.5 mL Reconstitution Solvent. Vortex-mix thoroughly. Transfer the contents to autosampler vials using glass transfer pipets, and then cap the vials.
3.2 Instrument Operating Conditions
1.The LC and MS operating conditions are given in Tables 2, 3, and 4 (see Note 4 ).Table 2LC operating conditions
Component
Parameter
Details
Binary pump
Gradient program
Time
Flow rate (μL/min)
%B
â0.0
350
ââ3
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